维药祖卡木颗粒剂澄清工艺的研究
颗粒,,祖卡木;工艺;高效液相色谱,1仪器与材料,2方法与结果,3小结,参考文献:
摘要:目的:评价三种天然澄清剂ZTC、101果汁澄清剂、壳聚糖与乙醇对维药祖卡木水提液的澄清效果。方法:通过用HPLC法测定祖卡木药液中大黄酚及甘草酸的含量,以有效成分的保留率及固形物收率为指标对4种澄清剂进行比较研究。结果:ZTC天然澄清剂、101果汁澄清剂、壳聚糖、乙醇澄清的药液中大黄酚的保留率分别为85.94%,86.64%,84.47%,89.67%。甘草酸的保留率分别为95.18%,83.30%,83.90%,81.82%。固形物收率分别为17.58%,16.23%,18.12%,17.04%。结论:澄清剂与乙醇沉淀法相比可提高有效成分含量,保持固形物的收率。关键词:祖卡木;工艺;高效液相色谱
Study on Clarifying Process of Zukamu Granule
CHEN Wen, YING Xue,JIANG Fashou, TANG Hui,LIU Xiao
(College of Pharmacy, Shihezi University, Shihezi 832002, China)
Abstract:Objective:To evaluate the clarifying effects of ZTC、101 juice chitosan natural clarifying agents and alcohol in Uigur medicine Zukamu decoction.Methods:The content of chrysophanol and glycyrrhizin in the residue received were considered with HPLC method . The rate of the available ingredients reserved and the residue received were considered as the standards to evaluate the clarifying effect of three natural clarifying agents.Results:The reserved rate of chrysophanol in the filtrate of ZTC、101 juice and chitosan were 85.94% ......
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