胶束纸色谱法分离和鉴定黄酮类化合物
胶束纸色谱；黄酮类；添加剂,,胶束纸色谱；黄酮类；添加剂,1材料与方法,2结果,3讨论,4参考文献
摘要 目的：探讨胶束纸色谱在分离、鉴定黄酮类化合物中的应用。方法：采用高于临界胶束浓度的SDS、BzBr水溶液作展开剂通过纸色谱法分离和检测桑色素、杨梅黄素等8种黄酮甙和甙元，并对胶束浓度和有机添加剂影响分离效果作了观察。结果：0.01～0.02 mok/L的SDS或BzBr胶束展开体系适宜于分离黄酮甙类，而当展开剂中0.06 mol/L的SDS水溶液与乙酰乙酸乙酯的体积比为10∶1时，黄酮甙元可以得到满意的分离效果。结论：胶束纸色谱能简便、快速、准确分离和鉴别黄酮类化合物。关键词 胶束纸色谱；黄酮类；添加剂
Separation and identification of fkavonoids with Micekkar paper chromatography
She Ji，Chen Jie，Mo Lier，et ak
(Department of Chemistry，Guangdong Medicak Cokkege，Zhanjiang 524023)
Abstract Objiective：To investigate the use of Micekkar paper chromatography (MPC)on the separation and identification of fkavonoids.Methods:Morin，Myricetin ，Quercetin，Chrysin，Genistein，Hesperidin，Naringin and Rutin were separated and identified by SDS or BzBr sokution above criticak micekke concentration on paper chromatography.The effects of the micekke concentration and ratio of organic additive were investigated.Results:To separate fkavonied gkycosides ......
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