高效液相色谱法测定舒金克喘胶囊中和厚朴酚与厚朴酚的含量
色谱,,舒金克喘胶囊；和厚朴酚；厚朴酚；高效液相色谱法,1仪器与药品,2方法与结果,3讨论,参考文献：
摘要：目的：测定舒金克喘胶囊中和厚朴酚与厚朴酚的含量。方法：色谱条件：色谱条件与系统适用性实验：Hypersil ODS2 C18分析柱(150 mm×4.6 mm，5 μm)；流动相：甲醇∶水=(78∶22)，检测波长294 nm，流速1.0 ml/min，室温操作。理论塔板数按厚朴酚计算应不低于3 000。结果：和厚朴酚与厚朴酚平均回收率分别为99.62%(RSD=1.34%)，98.56%(RSD=1.49%)。结论：方法快速准确,样品处理简便易行。关键词：舒金克喘胶囊；和厚朴酚；厚朴酚；高效液相色谱法
Determination of Magnolo and Honokiol in Shu Jin Ke Chuan Capsule by HPLC
KE Xuehong
(The First Affiliated Hospital, Guangzhou University of TCM, Guangzhou 510405, China)
Abstract:Objective:To determine the magnolo and honokiol in Shu Jin Ke Chuan Capsule.Methods:HPLC system consisted of Hypersil ODS 2 C18 column (125 mm×4.6 mm, 5 μm) Methanol:water=78∶22. As mobile phase, with detection wavelength at 294 nm, flow rate 1.0 ml/min.Results:For honokiol the mean recovery of 99.62% (RSD=1.34%), for Magnolo 98.56%(RSD=1.49%) for strychnine is obtained respectively.Conclusion:The method is sensitive, rapid and accurate.
Key words:Shu Jin Ke Chuan Capsule;Magnolo;Honokiol;HPLC
舒金克喘胶囊具有止咳、化痰、平喘等功效 ......
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