薄荷油；_β环糊精包合物；_正交实验；

薄荷油β环糊精包合物的制备工艺研究

http://www.100md.com 《时珍国医国药》 2005年第12期

薄荷油；,β环糊精包合物；,正交实验；,薄层色谱法；,显微影像,,薄荷油；,β环糊精包合物；,正交实验；,薄层色谱法；,显微影像,1仪器和试药,2方法与结果,3薄荷油β环糊精包合物薄层层析鉴别与显微成像鉴别,4讨论,参考文献：

     摘要：目的：研究薄荷油β环糊精包合物的最佳制备工艺。方法：用正交实验法研究配比、温度、时间三个因素对薄荷油β环糊精包合物的饱和水溶液法的制备工艺的影响，考察包合物的收率，并用TLC、显微影像验证包合物的形成。结果：最佳的工艺条件薄荷油2.5 ml，包合温度50℃，包合时间3.5 h。结论：此方法可用于制备薄荷油β环糊精包合物。

    关键词：薄荷油； β环糊精包合物；正交实验；薄层色谱法；显微影像

    Study on Preparation Procedure of βcyclodextrin Inclusion Compound for Pennyroyal

    ZHANG Xingsheng

    (Shenzhen Polytechnic Technology College, Shenzhen 518055, China)

    Abstract:Objective:To study optimum inclusion process for βcyclodextrin inclusion compound of Pennyroyal. Methods:The preparation procedure of βcyclodextrin inclusion compound of pennyroyal was studied by orthogonal test with 3 factors: Pennyroyal, temperature and time.The inclusion compound was proved by thin layer chromatography and microscope.Results:The optimum preparation conditions for inclusion compound were established as ：pennyroyal 2.5 ml ,inclusion temperature was at 50℃ and for 3.5hr. Conclusion:The method can be used for preparation of the inclusion compound. ......

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