表3 黄芪生脉饮中4种成分加样回收率试验

    成分原有量

    (μg)加入量

    (μg)测得量

    (μg)回收率

    (%)平均回

    收率(%)RSD

    (%)

    五味子乙素505.0215.6 718.9 99.76

    505.0215.6 719.9 99.90

    505.0431.3 898.3 95.9498.061.64

    505.0431.3 904.5 96.61

    505.0862.51342.4 98.16

    505.0862.51339.7 97.96

    五味子酯甲425.6184.4 593.7 97.33

    425.6184.4 591.5 96.97

    425.6368.8 787.1 99.0999.612.72

    425.6368.8 781.4 98.37

    425.6737.51191.7102.46

    425.6737.51203.9103.43

    党参炔苷143.723.8 165.9 99.04

    143.723.8 164.0 97.91

    143.747.5 189.9 99.3197.981.45

    143.747.5 189.3 98.97

    143.795.2 231.5 96.90

    143.795.2 228.7 95.73

    鲁斯可皂苷元811.8101.3 912.5 99.93

    811.8101.3 911.2 99.79

    811.8202.5 982.4 96.8599.301.25

    811.8202.51011.9 99.76

    811.8405.01207.6 99.24

    811.8405.01219.7100.24

    2.10 样品含量测定

    取5批黄芪生脉饮 ......